How Does The Isolation of 2 4-Di-tert-butylphenol and Butyrospermum 3 Take Place?

Posted on: May 4, 2022

Extraction And Isolation

In a study done, it was found that the isolation of 2 4, Di tert butylphenol and Butyrospermol is possible by using the stem bark of S.aquem. During the study, the powdered form of the stem bark of S.aqueuem was squashed by using 40 L of methanol at room temperature for a period of 3 days. The methanol extract was partitioned with n-hexane fraction separated by using a silica gel in gravity column chromatographic method with n-hexane. Ethyl acetate was used as an eluent. These similar fractions were then combined to obtain 19 fractions.

Result And Discussion

Compound 1(2mg) was collected as a yellow oil. Three protons showed in the aromatic protons region. The remaining 18 protons were identified as six methyls. After some time, COZY and HMBC correlations were joined together for confirmation of the structure. The NMR spectra were compared to previous literature. From this data compound, 1 was determined as 2 4-dtbp and the molecular formula was C14h220.

Compound 2 was obtained as a pale yellow oil. The proton signal at DH: 453ppm(C-3) belonged to the proton that was attached to the carbon that binds the ester group. The proton signal of 5.25(1H,m) and 5.12(1H,t, J=7.1 Hz) is linked to sp2 hybridized carbon. COZY and HMBC correlations were joined together for confirmation of the structure. NMR spectra were compared to previous literature data. From this data, compound 2 was identified as Butyrospermum. 3 palmitate and the molecular formula was C46H8002.

Conclusion

In this particular study, 96-76-4 butyl phenol and Butyspermol 3 palmitate were isolated from the stem bark of S.aquem. These phytochemical constituents are the first to be reported from the stem bark of this particular species.

About Vinati Organics

Vinati Organics is known as the world’s largest manufacturer of IBB and ATBS. We blend innovation with chemistry to deliver value-added products to our clientele. Our vision is to be the global leader in manufacturing niche specialty production by using eco-friendly technologies. Our mission is to emerge as a globally competitive organization for all our products in terms of cost and quality.

We have a market presence that spans more than 35 countries in the world. The company was founded in 1989 as a single product manufacturer and since then we have gone from strength to strength and are now an integrated business that offers a wide range of products which including di tert butyl phenol to some of the biggest chemical companies across the US, Europe, and Asia.

We offer a wide range of organic chemicals, specialty chemicals, and niche specialty chemicals to customers spread across the globe.

Our research and development capabilities and expertise to manufacture superior quality and cost-effective chemicals have kept us ahead of the industry curve. All our investments are in research and development specifically aimed at modifying the use of catalysts, equipment processes, and operating systems. To further strengthen our commitment to making a sustainable difference, we invest in technologies that can mitigate the impact of climate change and enable us to develop green chemistry.

Through our hard work, we have achieved global benchmarks for the highest purity standards like

  1. Our ATBS product has successfully achieved a high purity standard with a purity tolerance of 0.5% as against the global acceptance tolerance level of 3%.
  2. Our IBB product achieved a 99.7% purity standard which is the highest in the world.
  3. Our IB product has also achieved a 99.85% purity which is also the highest in the world.
  4. Our HP-MTBE product has achieved a purity of 99.97% which is once again the highest in the world.